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7390427 |
Hydrofluoroether as a heat-transfer fluid
The present invention provides an apparatus comprising a device and a mechanism for heat transfer comprising a hydrofluoroether heat-transfer fluid wherein the heat transfer fluid is represented by...
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7375254 |
Process for recovery of 1,1,1,3,3,3-hexafluoroisopropanol from the waste stream of sevoflurane synthesis
Provided is a process of obtaining 1,1,1,3,3,3-hexafluoro-2-propanol (“HFIP”) from a composition comprising an HFIP hydrolyzable precursor. The HFIP hydrolyzable precursor is a compound, other...
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7288682 |
Separation of bifunctional perfluoropolyethers (PFPEs) having -CH2OH termination from their mixtures with -CH2OH monofunctional PFPEs
A process for separating bifunctional perfluoropolyethers (PFPEs) having two terminations —CH 2 OH from their mixtures with monofunctional PFPEs with one termination —CH 2 OH, of general...
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7247757 |
Method of producing a fluorine-containing vinyl ether compound
A method of producing a fluorine-containing vinyl ether compound, which contains the step of: fluorinating a compound of formula (I-1) or (I-2):
wherein R is a straight-chain, branched-chain or...
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7230147 |
Process for functionalizing a double bond
The invention concerns a method for functionalizing a double bond and, more particularly, a double bond bearing a metalloid atom. Said functionalization is produced by the action of perhalogenated...
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7230143 |
Chromatographic method for the analysis of both in process and finished sevoflurane
A method in which organic matter found in a crude sevoflurane may be separated, identified, and quantified using a CARBOWAX™ (polyethylene glycol) capillary gas chromatographic column or an alkyl...
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7230142 |
Process for purifying fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether
A process for purifying fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether containing at least 1,1,1,3,3,3-hexafluoroisopropyl alcohol. The purifying process comprises the treatment of causing...
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7202386 |
Method for the preparation of sevoflurane
A method for the preparation of sevoflurane which comprises (a) providing a liquid mixture of (CF 3 ) 2 CHOCH 2 Cl, hydrogen fluoride, and an amine and (b) reacting the mixture, to form (CF 3 ) 2...
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7193119 |
Process for producing fluorinated alkyl ether
To provide a process for producing a fluorinated alkyl ether, whereby a sufficient reaction rate can be attained even under mild reaction conditions, and a post-process such as distillation after...
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7193118 |
Method for producing fluoroalkyl ether
A method for producing a fluoroalkyl ether, which comprises reacting a fluoroalkyl alcohol with a fluorinated olefin in the presence of a solvent and a catalyst, wherein the fluoroalkyl alcohol and...
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7153397 |
Process for the purification of fluoromethyl hexafluoroisopropyl ether
A process for the purification of fluoromethyl hexafluoroisopropyl ether which comprises contacting a crude composition comprising fluoromethyl hexafluoroisopropyl ether and hexafluoroisopropyl...
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7141704 |
Process for preparing hydrofluoroethers
Process for obtaining hydrofluoroethers of formula (I):
A-(R f ) n0 —CF(R f1 )—O—R h (I)
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7128133 |
Hydrofluoroether as a heat-transfer fluid
The present invention provides an apparatus comprising a device and a mechanism for heat transfer comprising a hydrofluoroether heat-transfer fluid wherein the heat transfer fluid is represented by...
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7125834 |
Functional substances derived from oligoolefins having functional groups at the ends
This invention provides the following: an amphiphilic functional substance with lipophilicity, affinity for supercritical CO 2 , and if necessary hydrophilicity comprising an oligoolefin chain and...
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7102031 |
Method for producing diene compound
It is an object to obtain from a mixture of a specific diene compound (1) and a compound (2) with the same molecular weight and molecular formula hard to separate by distillation, the diene...
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7091374 |
Fluorinated compounds
Fluorinated compounds and emulsions including the compounds. The compositions are useful as oxygen carriers and surfactants. In one embodiment, the fluorinated compound is pH sensitive. In one...
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7060850 |
Fluorous tagging and scavenging reactants and methods of synthesis and use thereof
The present invention includes methods and compositions for increasing the fluorous nature of an organic compound by reacting it with at least one fluorous compound to produce a fluorous tagged...
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7034190 |
Process for the production of fluoromethyl hexafluoroisopropyl ether
A process for the production of fluoromethylhexafluoroisopropylether which comprises contacting bis(fluoromethyl)ether with hexafluoroisopropyl alcohol in which the molar ratio of the ether to...
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7019178 |
Process for the purification of fluoromethyl hexafluoroisopropyl ether
A process for the purification of fluoromethyl hexafluoroisopropyl ether involving contacting a crude composition containing impure fluoromethyl hexafluoroisopropyl ether with an adsorbent having...
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6911513 |
Fluorinated diene compound and fluoropolymer, and methods for their production
A novel fluoropolymer which can be an optical resin material having a low refractive index and excellent heat resistance, and a novel fluorinated diene compound having two unsaturated bonds,...
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6849194 |
Methods for preparing ethers, ether compositions, fluoroether fire extinguishing systems, mixtures and methods
Highly fluorinated, saturated, and unsaturated fluoroethers are efficient, economical, non-ozone-depleting fire extinguishing agents used alone or in blends with other fire extinguishing agents in...
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6800786 |
Preparation of desflurane
Provided is a method for the preparation of desflurane wherein isoflurane is reacted with 0.7-1.2 mol. % of antimony pentachloride and 1.3-2.2 molar equivalents of hydrogen fluoride. Typically, the...
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6770776 |
Synthesis of fluorocarbon compounds
Fluorocarbon compounds are synthesized by reacting a substrate hydrocarbyl compound containing at least one sp 3 -hybridized halophoric carbon atom bearing at least two halogen atom substituents,...
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6756458 |
Fluorinated compound, method for its production and polymer thereof
A novel polymer useful as an optical resin material excellent in heat resistance, a novel monomer for obtaining the polymer, etc., are provided. A fluorinated diene represented by CF 2 ═CF(CF 2 )...
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6677492 |
Fluoroether compositions and methods for inhibiting their degradation in the presence of a Lewis acid
The present invention relates to an anesthetic composition containing a fluoroether compound and a physiologically acceptable Lewis acid inhibitor. This composition exhibits improved stability and...
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6670511 |
Fluorine-containing diene, its production method and its polymer
A fluorine-containing diene represented by the formula 1: CF 2 ═CF(CF 2 ) n CXYOCF═CF 2 Formula 1 wherein each of X and Y which are independent of each other, is an atom selected from a...
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6509509 |
Process for the preparation of perfluoropolyoxyalkylenes with hydroxyl end groups
A process for preparing perfluoropolyoxyalkylenes with hydroxyl end groups having structure: T 1 —CFW 1 —O—R f —CFW 2 —T 2 (I) wherein: T 1 , T 2 , are selected from —CH 2 OH, —F,...
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6469219 |
Production of fluoromethyl 2,2,2-trifluoro-1-(trifluoromethyl)ethyl ether
An improved process for preparing fluoromethyl 2,2,2-trifluoro-1-(trifluoromethyl)ethyl ether(sevoflurane) by reacting 1,1,1,3,3,3-hexafluoro-2-propanol with formaldahyde and hydrogen fluoride...
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6448451 |
Process for removal of dimethyl ether in the synthesis of sevoflurane
The invention provides a process for purifying methyl 2,2,2-trifluoro-1-(trifluoromethyl)ethyl ether, comprising: passing a composition comprising methyl 2,2,2-trifluoro-1-(trifluoromethyl)ethyl...
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6365769 |
Perfluoroalkyl halides and derivatives
Novel mixtures of perfluoroalkyl halides and derivatives thereof are described. These mixtures contain some compounds with a straight perfluoroalkyl group and some with a branched perfluoroalkyl...
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6315869 |
Process for purification of perfluorovinyl ethers
A perfluorovinyl ether of the formula: RfO(CF 2 CFXO) n CFCF 2 (1) in which Rf is a perfluoralkyl group, X is a fluorine atom or a trifluoromethyl group, and n is a number of 0 to 20...
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6303831 |
Synthetic method for fluoromethylation of halogenated alcohols
A method for fluoromethylation of a halogenated alcohol. The method includes refluxing a halogenated alcohol with a dihalomethane under basic conditions in a first solvent to form a halomethyl...
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6300526 |
Hydro-fluoroalkylvinylethers and process for obtaining them
Hydro-2,2-difluoroalkylvinylethers having the formula CF 2 CH--O--R A (I) wherein R A is a radical containing fluorine, optionally containing halogens such as Cl, Br, I, hydrogen,...
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6271422 |
Method for fluoromethylation of alcohols via halogenative decarboxylation
A method for fluoromethylation of an alcohol via halogenative decarboxylation. The method includes the step of reacting an alcohol of the formula R 1 C(CX 3 ) 2 OH with an alpha-haloester of the...
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6245949 |
Synthetic method for the fluoromethylation of alcohols
A method for fluoromethylating halogenated alcohols. The method includes the step of providing an alpha-halogenated alcohol of the formula R 1 C(CX 3 ) 2 OH, wherein R 1 is selected from the...
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6225511 |
Synthesis of fluorinated ethers
Fluorinated ethers of the formula: ##STR1## wherein R is hydrogen, fluorine, alkyl of 1 to 6 carbon atoms, or fluoroalkyl of 1 to 6 carbon atoms, R' is hydrogen, alkyl of 1 to 6 carbon atoms, or...
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6100434 |
Method for synthesizing sevoflurane and an intermediate thereof
A method for synthesizing fluoromethyl-1,1,1,3,3,3-hexafluoroisopropyl ether. The method includes the step of combining in the presence of aluminum trichloride a quantity of hexafluoroisopropanol...
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6072088 |
Chemical compounds having two trifluoromethyl groups
A compound having the formula: CF 3 CH 2 -w (H 1 -x CH 2 -y R m R' n CH 1 -z) p H 2 -q CF 3 wherein w=0, 1 or 2; x=0 or 1; y=0, 1 or 2; m=0, 1 or 2; n=0 or 1; z=0 or 1; p=1 or 2; and q=0, 1...
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6046368 |
Catalytic process for making hydrofluoroethers
Briefly, in one aspect, this invention provides a catalytic method of preparation of primary and secondary hydrofluoroethers, the process comprising reacting a fluorinated precursor material and an...
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6023002 |
Process for preparing hydrofluoroethers
Described is a reaction of a fluorinated alkoxide with an alkyl fluorovinylalkyl ether, the alkyl fluorovinylalkyl ether having alpha-beta carbon-carbon unsaturation relative to the ether oxygen,...
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6019909 |
Fluorinated hydrocarbon compound and process for its preparation, and refrigerator oil and magnetic recording medium lubricant
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5990359 |
Process for the production of fluoromethylhexafluoroisopropylether
Process for producing Sevoflurane anaesthetic which comprises reacting hexafluoroisopropyl alcohol with essentially pure bis(fluoromethyl)ether. The bis(fluoromethyl)ether is preferably obtained by...
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5965779 |
Fluorooxetane compound and process for its preparation
The present invention provides processes for preparing 2,2,3,3,4-pentafluorooxetane and/or 2,2,3,3,4,4-hexafluorooxetane which comprises reacting 2,2,3,3-tetrafluorooxetane with fluorine gas, the...
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5917008 |
Polytetrafluoroethylene dispersions in an organic solvent and dispersing agents employed therein
Polytetrafluoroethylene (PTFE) dispersions in an organic solvent, comprising: (A) from 2 to 40% by weight of PTFE in powder form; (B) from 50 to 95% by weight of an organic solvent; (C) from 0.5 to...
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5886239 |
Method of preparing monofluoromethyl ethers
A method of preparing fluoromethyl 2,2,2-trifluoro-1-(trifluoromethyl)ethyl ether (sevoflurane) and structurally related monofluoromethyl ethers in which the monochloromethyl ether precursor...
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5856587 |
Flame extinguishing compositions
Extinguishing compositions comprising a liquid extinguishing agent constituted by hydrofluoropolyethers having general formula HF 2 CO(CF 2 O) n (CF 2 CF 2 O) m CF 2 H wherein n and m are...
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5811596 |
Method of producing fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether
The present invention provides a novel method of producing fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether. It is a method of producing fluoromethyl 1,1,1,3,3,3-hexafluoroisopropyl ether by...
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5763684 |
Method of purifying fluoromethyl-1,1,1,3,3,3-hexafluoroisopropyl ether
The present invention relates to a method of removing bisfluoromethyl ether contained in fluoromethyl-1,1,1,3,3,3-hexafluoroisopropyl ether in a simple, effective manner, and is characterized in...
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5753776 |
Liquid-phase fluorination
This invention pertains to a method for liquid phase fluorination for perfluorination of a wide variety of hydrogen-containing compounds.
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5750807 |
Production of hyrofluorocarbons
A process for the production of a hydro(halo)fluorocarbon which comprises heating an α-fluoroether in the vapor phase at elevated temperature. α-fluoroethers are obtained by reacting a...
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