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6254850 |
Metal complexes, suitable for use in diagnosis and therapy
The invention relates to diethylenetriaminepentaacetic acid derivatives, their complexes and complex salts, containing an element of atomic numbers 20-32, 39-51 or 57-83, pharmaceutical agents...
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6229011 |
N-aroylphenylalanine derivative VCAM-1 inhibitors
Compounds of the formula: ##STR1## are disclosed which have activity as inhibitors of binding between VCAM-1 and cells expressing VLA-4. Such compounds are useful for treating diseases whose...
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6040432 |
Metal complexes, of DTPA derivatives suitable for use in diagnosis and therapy
The invention relates to diethylenetriaminepentaacetic acid derivatives, their complexes and complex salts, containing an element of atomic numbers 20-32, 39-51 or 57-83, pharmaceutical agents...
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6017918 |
Phenyl glycine compounds and methods of treating atherosclerosis and restenosis
The present invention provides compounds having the Formula I ##STR1## The present invention also provides methods of treating atherosclerosis, coronary heart disease, and restenosis using the...
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5658943 |
Phenylalanine derivatives as endothelin antagonists
Novel antagonists of endothelin are described, as well as novel intermediates used in their preparation, methods for the preparation and pharmaceutical compositions of the same, which are useful in...
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5510522 |
Synthesis of N-formyl-3,4-di-t-butoxycarbonyloxy-6-(trimethylstannyl)-L-phenylalanine ethyl ester and its regioselective radiofluorodestannylation to 6- .sup.18 F!fluoro-1-dopa
A process for forming a 6-fluoro derivative of compounds in the L-Dopa family comprising the steps of protecting the groups attached to the benzene ring in the compound followed by serially...
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5338859 |
Process for the production of calcium salts of hydantoic acids
The present invention provides a process for the production of calcium salts of hydantoic acids and which comprises the steps of reacting a hydantoin with a calcium base material such as calcium...
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5288898 |
N-methylphenylserine alkyl ester derivatives and uses thereof
As new compounds are now provided N-methyl-3-(3,4-dihydroxyphenyl)serine alkyl esters which are effective as an α-adrenergic and β-adrenergic agent to stimulate the α-adrenergic and...
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5254726 |
No-carrier-added (NCA) aryl (18E) fluorides via the nucleophilic aromatic substitution of electron rich aromatic rings
A method for synthesizing no-carrier-added (NCA) aryl [ 18 F] fluoride substituted aromatic aldehyde compositions bearing an electron donating group is described. The method of the present...
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5246943 |
Substituted 1,2,3,4-tetahydroisoquinolines with angiotensin II receptor antagonist properties
This invention relates to novel substituted 1,2,3,4-tetrahydroisoquinolines which are useful in the treatment of vascular restenosis, various disorders of the central nervous system, in the...
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5194663 |
Aromatic derivatives of butyric acid, a process for their preparation and their use in cosmetics and in human and veterinary medicine
An aromatic derivative of butyric acid has the formula ##STR1## These aromatic derivatives of butyric acid are useful in human and veterinary medicines as well as in cosmetic compositions.
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5041637 |
Process for the synthesis of optically active aminoacids
New process for the synthesis of optically active aminoacids of formula ##STR1## by treating compounds of formula ##STR2## which an optically active alcohol of formula R 4 --OH ...
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5013868 |
Process for treating amphoteric amino acids
The present invention relates to a process for treating amphoteric amino acids, and/or amphoteric amino acid derivatives in a fluid bed, whereby in order to maintain fluidizing conditions one adds...
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4962223 |
Process for the synthesis of the levodopa
New process for the synthesis of the levodopa, L-(-)-2-amino-3-(3,4-dihydyphenyl)propionic acid, drug used in the treatment of the Parkinson's disease. The process consists in resolving with...
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4929755 |
Process for making an optically active mixture of an N-acyl-amino acid or ester containing at least two chiral centers
In the process of hydrocarboxylating an α-enamide with CO and H 2 O or an organic hydroxyl compound to produce an N-acyl-α-amino acid or ester, respectively, the improvement comprising using as...
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4888043 |
Herbicidal amino-mesityl cyclohexane-1,3-dione compounds
The invention concerns compounds of the formula I ##STR1## wherein: Z is selected from hydrogen, alkyl, alkanoyl, sulfamoyl, carboxy and trifluoroacetamido; Y is selected from various carboxy or...
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4879398 |
Process for producing 2,6-disubstituted tyrosine
A process for making 2,6-disubstituted tyrosine by the noble metal coupling of a disubstituted aromatic halide or diazonium salt with an amino-protected 2-aminoacrylic acid to form a...
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4837332 |
Process for blocking amino acids with the tertiary-alkoxycarbonyl group
Amino acid salt having at least one unblocked amino group and comprising at least one cation which has a nitrogen cationic atom is reacted with 1-(tertiary-alkoxycarbonyl)imidazole in the liquid...
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4833273 |
Process for the resolution of 1-aminoindanes
An improved process for the resolution of 1-aminoindanes into the R-isomer on a large scale is described. The resolving agent used in the process is R-N-acetyl-3,4-dimethoxyphenylalanine. The...
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4769486 |
Method for racemizing an optically active amino acid
A method for racemizing an optically active amino acid, which comprises heating the optically active amino acid in an aqueous solution under an alkaline condition in the presence of an alkali metal...
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4740615 |
Process for purified amino acids
A process for the recovery in substantially pure form of an amino acid represented by the formula ##STR1## from an aqueous production mixture by a low pressure temperature gradient chromatographic...
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4716246 |
Process for L-dopa
A process for the preparation of (S)- or L-3-(3,4-dihydroxyphenyl)alanine (L-dopa) is described. The process utilizes water as reaction process solvent and proceeds via formation of an intermediate...
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4695588 |
Fluorinated amino acids
Novel substituted α-fluoromethyl-α-amino alkanoic acids and esters thereof are disclosed. The novel compounds have biological activity including decarboxylase inhibition.
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4675439 |
Preparation process of N-acylphenylalanines
A process for preparing an N-acylphenylalanine represented by the formula (II): ##STR1## wherein R 3 and R 4 mean individually a hydrogen atom or an alkyl, alkoxy, phenoxy, hydroxy or...
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4661510 |
α-allenic-α-amino acids as enzyme inhibitors
Novel α-allenic-α-amino acids which are enzyme inhibitors of the suicide or k cat type are disclosed herein.
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4638086 |
Process for the racemization of optically active aminoacids
The racemization of optically active aminoacids (including their N-acyl derivatives) by heating with carboxylic acids takes place particularly readily with carboxylic acids of low volatility. Only...
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4634775 |
Optically active 3,4-bis-(diphenylphosphino)-pyrrolidine, and rhodium complexes, containing it as chiral ligands
There are described new optically active 3,4-bis-(diphenylphosphino)-pyrrolidines of the formula ##STR1## wherein Ph is a phenyl group and R is hydrogen, an alkyl group, an arylalkyl group or an...
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4613691 |
Preparation of amino acids from unsaturated hydantoins
Amino acids can be easily prepared by reducing unsaturated hydantoins to the corresponding saturated hydantoins by hydrogenating the unsaturated hydantoin using either Raney Nickel catalyst in the...
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4612388 |
Process for producing N-acylphenylalanines
Disclosed herein is a process for producing an N-acyl-substituted or unsubstituted phenylalanine comprising hydrolyzing a 2-substituted-4-substituted or unsubstituted benzylidene-5-oxazolone with...
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4508921 |
Process for preparation of alpha-alkyl amino acids
A process for preparing α-alkyl amino acids by enantioretentive α-alkylation of α-amino acids is described. The products are bioactive compounds including some useful as therapeutic agents.
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4480109 |
Process for producing threo-3-(3,4-dihydroxyphenyl)serine
A process for producing an optically active threo-3-(3,4-dihydroxyphenyl)serine represented by the formula ##STR1## which is useful as a remedy for peripheral orthostatic hypotension or as an...
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4452783 |
Derivatives of substituted phenylacetic acids and compositions containing them
Aminoacid and peptide derivatives of the formula: A--NH--R 1 --CO] x [NH--R 2 --CO] y NH--R 4 --COOH in which A, R 1 , R 2 , x and y have the meanings specified in claim 1 for formula I, and...
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4453007 |
Method for increasing the purity of amphoteric compound compositions
Provided is a method of increasing the purity of amphoteric compound compositions. The method is: (a) providing an amount of a crude amphoteric compound composition, (b) using a portion of the...
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4440936 |
Rhodium-phosphine chiral hydrogenation catalysis of acetophenone, atropic acid, and alpha-acylamidoacrylic acids and esters thereof
The chiral phosphine ligand (R)-1,2-bis(diphenylphosphino)-1-cyclohexylethane, when complexed to Rh(I), functions as a superior chiral hydrogenation catalyst. The chiral phosphine ligand is more...
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4436910 |
Process for the production of aqueous solutions of sodium salts of α- a
Aqueous solutions of sodium salts of α-aminocarboxylic acids practically free of foreign salts are produced by saponifying the corresponding hydantoin at a temperature between 110° C. and 180°...
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4421767 |
Compounds and methods for treating depression
Compounds of the formula: ##STR1## wherein: X is fluorine, chlorine, or bromine; R is the group R 2 as defined below; R 1 is a group of the formula: ##STR2## or the group R 2 as defined...
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4404392 |
Resolution of α-pivaloyloxyethyl-(S)-3-(3,4-dihydroxyphenyl)-2-methylalantinate into its α and β isomers
Resolution of the α and β isomers of α-pivaloyloxyethyl-(S)-3-(3,6-dihydroxyphenyl)-2-methylalan
inate is accomplished by; (a) forming the (+) hydrogen tartrate salt of the mixture; (b)...
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4401676 |
Novel α-amino acids
Novel α-ethynyl- and α-vinyl 3,4-disubstituted phenylalanines are disclosed. The compounds have pharmaceutical activity.
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4380646 |
Method for the N-acylation of aminocarboxylic acids
A process is disclosed for the prparation of an acylated aminocarboxylic acid which comprises contacting an aminocarboxylic acid, its alkali metal or alkaline earth metal salt with a low alkyl...
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4339589 |
Preparation of 4-substituted oxazolidin-5-ones
Manufacture of 4-substituted oxazolinone-(5) compounds, which are intermediates for substituted aminoacids, by alkylation of 2-substituted or 3,4-disubstituted oxazolinone-(5) compounds in an...
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4288601 |
Fluorination process
A process for preparing α-fluoromethyl amino acids is disclosed. The process utilizes SF 4 and BF 3 or AlCl 3 in HF to effect the fluorination.
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4264771 |
Alkylation of substituted oxazolinone-(5) compounds
Manufacture of 4-substituted oxazolinone-(5) compounds, which are intermediates for α-substituted aminoacids, by alkylation of 2-substituted or 3,4-disubstituted oxozolinone-(5) compounds in an...
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4230893 |
1,1-Di(4-hydroxy-3-methoxyphenyl)-2-alkoxypropane
4-Hydroxy-3-methoxyphenylacetone, an intermediate for methyldopa, has been prepared from reacting two moles of guaiacol and one mole of a 2-alkoxy propanol followed by basic elimination to form the...
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4124533 |
Metal coordination complexes containing optically active phosphine or arsine ligands
Process for the homogeneous catalytic hydrogenation of β-substituted-α-acylamido-acrylic acids which yields, after hydrogenation, an optically active mixture. The process comprises the...
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4120867 |
Monoradioiodinated phenolic esters, acids and amines
Monoradioiodinated derivatives of compounds employed in a radioassay prepared from precursors which are either active esters, amino acids, or amines, including a phenolic or imidazole substituent...
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4111933 |
Protection of functional groups during reaction and their subsequent restoration
In the process for preparing an organic compound of the formula A' -- X in which X is an amino group, a hydroxyl group or a carboxyl group, and A' is the remainder of the molecule, from an...
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4087520 |
Lowering blood pressure with new L-3-(3,4-dihydroxyphenyl)-2-methyl-alanine peptides
An L-3-(3,4-dihydroxyphenyl)-2-methyl-alanine peptide of the formula ##STR1## wherein A is an alkylene radical which can be substituted by a hydroxyl group or by a phenyl radical which optionally...
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4020060 |
7-[α-Amino- ω-(3,4-methylenedioxyphenyl)acylamido]cephalosporanic acid derivatives
Novel 7-[α-amino-ω-(3,4-methylenedioxyphenyl)acylamido]cephalosp
oran ic acid derivatives are prepared which are useful as antibacterial agents.
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4010181 |
Process for the asymmetric hydrogenation of a substituted acrylic acid or ester thereof
Optically active diphosphines of the formula, ##STR1## in which the phosphinomethyl groups are trans to each other, form rhodium complexes useful as catalysts in hydrogenating substituted acrylic...
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4005127 |
L-Dopa process and intermediates
A process for the preparation of 3-(3,4-dihydroxyphenyl)-L-alanine (L-DOPA) wherein α-acetamido-4-hydroxy-3-alkoxy-cinnamic acid acetate is subjected to catalytic asymmetric hydrogenation to yield...
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