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8110704 |
Process for the production of stable polymers
Stable NCO prepolymers are produced from polyisocyanates having a melting point greater than 70° C., preferably, naphthalene diisocyanate, having advantageous physical properties. An important ...
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8088944 |
Method for the purification of isocyanates
Isocyanates are prepared by a process in which a product stream from the isocyanate synthesis is purified.
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8063241 |
Process for the preparation of toluene-diisocyanate
The present invention relates to a process for the preparation of toluene-diisocyanate. In this process, toluenediamine is reacted with phosgene to give crude toluene-diisocyanate, the crude...
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8034972 |
System and process for production of toluene diisocyanate
A method for producing toluene diisocyanate is disclosed which comprises forming a dispersion comprising phosgene gas bubbles dispersed in toluene diamine liquid phase, wherein said gas bubbles...
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7842277 |
Molecular sieve composition, a method of making and a process of using the same
This disclosure relates to a crystalline MCM-22 family molecular sieve composition having, in its as-synthesized form, an X-ray diffraction pattern including a peak at d-spacing maximum of...
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7649108 |
Process for the distillation of a mixture of isomeric diisocyanatodiphenylmethanes
A mixture of isomeric diisocyanatodiphenylmethanes composed of at least 2,2′-diisocyanato-diphenylmethane, 2,4′-diisocyanatodiphenylmethane and 4,4′-diisocyanatodiphenyl-methane is distilled in at...
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7645900 |
Process for the preparation of isocyanates
The present invention relates to a process for the preparation of isocyanates by reacting the appropriate amines with phosgene, condensing the gas mixture thereby obtained, stripping the liquid...
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7615662 |
Process for the preparation of isocyanates in the gas phase
Isocyanates are produced by reaction of primary amines with phosgene in the gas phase. In this process, the reaction is terminated by guiding the reaction mixture from the reaction chamber through...
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7595422 |
Process for conditioning isocyanates
The invention relates to a novel process for conditioning isocyanates. The purpose of conditioning of isocyanates or of mixtures of isocyanates is to remove organophosphorus components in a...
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7592479 |
Reprocessing of reaction material discharged from phosgenation reactors
Isocyanates are prepared by reacting primary amines with phosgene in a reactor by a process in which a reaction discharge is present in the form of a suspension which contains the isocyanate to be...
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7544832 |
Reaction column in a special combination with a natural circulation evaporator
An arrangement for carrying out chemical reactions comprises at least one distillation column and/or at least one container and at least one circulation evaporator, which are connected to one...
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7524405 |
Method for separating out solvent from a reaction mixture resulting from an isocyanate synthesis and for purifying this solvent
The invention relates to a process for preparing isocyanates by reaction of amines with phosgene in the presence of inert organic solvents in a reactor and subsequent work-up of the reaction...
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7504533 |
Process for the production of isocyanates
Isocyanates are produced by a) reacting at least one amine with phosgene, optionally in the presence of a solvent to produce the corresponding isocyanate and a stream containing hydrogen chloride,...
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7495124 |
Process for the production of very pure 2,4′-methylenediphenyl diisocyanate
The present invention relates to a process for the production of MDI fractions containing 2,4′-MDI, and in which the 2,2′-MDI component from the MDA production is largely removed from the iso...
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7358388 |
Method for the purification of isocyanates
Isocyanates are prepared by a process in which a product stream from the isocyanate synthesis is purified.
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7205430 |
Production of di- and polyisocyanates of the diphenylmethane series with defined acidity
The invention relates to a process for the production of di- and polyisocyanates of the diphenylmethane series and mixtures thereof, in which aniline and formaldehyde are reacted in the presence of...
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7118653 |
Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column
Process for the purification of toluenediisocyanate from a crude distillation feed which includes toluenediisocyanate, an organic solvent and less than 2% by weight phosgene by separating the crude...
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7108770 |
Process for the purification of toluene diisocyanate incorporating a dividing-wall distillation column for the final purification
Toluene diisocyanate is recovered from a crude distillation feed containing less than 2% by weight of phosgene by (a) fractionating the crude distillation feed containing less than 2% by weight of...
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6982026 |
Azeotropic distillation process for producing organic acids or organic acid amides
Disclosed herein are methods for the recovery of at least one of an organic acid or an organic acid amide, such as a heat stable lactic acid or lactamide, from a feed stream which contains the...
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6966992 |
Method of purification of molecules using unbranched terminal alkyldiols
The current invention provides methods for molecule purification by RP-LC and RP-HPLC that uses unbranched terminal alkyldiols as eluting solvents. In particular, the present invention purifies...
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6803483 |
Process for the purification of mixtures of toluenediisocyanate
A process for the purification of toluenediisocyanate by fractionating a crude distillation feed containing toluenediisocyante, an organic solvent and less than 2% by weight of phosgene in a heat...
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6800781 |
Process for quenching a gaseous reaction mixture during the gas phase phosgenation of diamines
The present invention provides a process for quenching a gaseous reaction mixture during the phosgenation of diamines in the gas phase to produce diisocyanates. The gaseous reaction mixture...
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6673960 |
Work-up of distillation residues from the synthesis of toluene diisocyanate
A process for working up distillation residues from the synthesis of tolylene diisocyanate by reaction of the distillation residues with water comprises reacting the TDI distillation residues with...
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6664415 |
Process for preparing organic monoisocyanates
The present invention relates to a process for preparing a low boiling monoisocyanate having a boiling point of between 70 and 320° C. at standard pressure by reacting A) a high boiling isocyanate ...
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6639102 |
Process for producing polyisocyanates of the diphenyl methane series having a reduced color value
Polyisocyanates of the diphenyl methane series having reduced color values are obtained by a) reacting aniline and formaldehyde in the presence of an acid catalyst to form a polyamine, b)...
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6576788 |
METHOD FOR PRODUCING MIXTURES CONSISTING OF DIPHENYLMETHANE DIISOCYANATES AND POLYPHENYLENE-POLYMETHYLENE-POLYISOCYANATES CONTAINING A REDUCED AMOUNT OF CHLORINATED SECONDARY PRODUCTS AND WITH A REDUCED IODINE COLOR INDEX
In a process for preparing mixtures of diphenylmethane diisocyanates and polyphenylpolymethylene polyisocyanates having a reduced content of chlorinated by-products and a reduced iodine color...
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6395925 |
Process for purifying organic isocyanates, the organic isocyanates so purified and their use
The invention provides a new process for purifying organic isocyanates or isocyanate mixtures by mixing the isocyanates or isocyanate mixtures to be purified with at least one alcohol and/or thiol...
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6391161 |
Method for reducing the chlorine content of low molecular weight isocyanates
An organic isocyanate or mixture of isocyanates is treated with at least one high molecular weight ester of phosphoric acid corresponding to a specified formula to remove chlorine compounds. The...
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6271414 |
Process for the isomeric separation of isocyanates
A process is described for obtaining pure isocyanate isomers from a mixture of isocyanate isomers by suspension crystallization and the isolation of isomerically pure crystals, which is...
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6229043 |
Preparation of mixtures of diphenylmethane diisocyanates and polyphenylpolymethylene polyisocyanates having a reduced iodine color number and a reduced chlorine content
Mixtures of diphenylmethane diisocyanates and polyphenylpolymethylene polyisocyanates (raw MDI) having a reduced iodine color number and a reduced chlorine content are prepared by reacting the...
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6222066 |
Process for decreasing the chlorine content of organic isocyanates
A process for the purification of organic isocyanates or isocyanate mixtures in which the amount of chlorine compound(s) present is reduced by mixing the isocyanate(s) or isocyanate mixtures with a...
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6140382 |
Process for the preparation of isocyanates or isocyanate mixtures useful for the preparation of polyurethane foams
Isocyanates or isocyanate mixtures which are substantially free of color-imparting components are made by treating the isocyanate with hydrogen in the presence of a catalyst at a pressure of from...
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5962728 |
Isocyanate residue purification
The present invention relates to a process for isolating aliphatic isocyanate monomer(s) from a liquid or viscous paste composition comprising polymeric isocyanate residues and the aliphatic...
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5889070 |
Process for preparing polyamines and polysocyanates
Disclosed herein is an improved process for preparing a polyamine mixture derived by reacting aniline with formaldehyde in the presence of an acid catalyst the improvement comprising mildly...
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5786506 |
Process for distillation of crude isocyanate concentrates
A process is described for the separation and recovery of isocyanate monomers from isocyanate concentrates which leaves a residue which is liquid and burnable. The process for the separation and...
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5783727 |
Production of 2,6-toluylene diisocyanate from a mixture comprising 2,6-toluylene diisocyanate and 2,4-toluylene diisocyanate
A method for obtaining substantially pure toluylene 2,6-diisocyanate from a mixture of the 2,4 and 2,6 isomers of toluylene diisocyanate, wherein at least one crystallizing-melting cycle is...
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5750629 |
Uretdione diisocyanates and a process for their production
The present invention relates to a process for preparing pure bis(isocyanatoalkyl)monouretdiones corresponding to formula (I) ##STR1## wherein R represents identical or different, linear or...
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5703193 |
Removal of unreacted diisocyanate monomer from polyurethane prepolymers
A process for reducing the amount of residual organic diisocyanate monomer in a polyurethane prepolymer reaction product mixture which comprises distilling the polyurethane prepolymer reaction...
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5606001 |
Polyisocyanates containing allophanate groups and optionally isocyanurate groups
The present invention relates to a polyisocyanates containing allophanate groups and optionally isocyanurate groups that are prepared by reacting compounds which i) are substantially free of...
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5451697 |
Process for preparing isocyanates
A process for preparing isocyanates comprising contacting carbon dioxide and a primary amine in the presence of an aprotic organic solvent and a base selected from the group consisting of a...
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5446196 |
Process for the production of isocyanates and for the continuous working-up of the residue
Pure isocyanate is recovered from an isocyanate-containing residue of a phosgene/amine reaction mixture by continuously feeding such residue and a high boiling hydrocarbon such as bitumen to a...
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5386054 |
Process for the purification of polyisocyanates, the polyisocyanates thus purified and use thereof
A process for the purification of organic polyisocyanates by mixing of the polyisocyanate with from 0.001 to 1% by weight of compounds containing trimethylsilyl groups at temperatures of from 20° ...
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5364958 |
Process for the production of methylene-crosslinked polyphenylene polyisocyanate
The hue of a methylene-crosslinked polyphenylene polyisocyanate continuously produced by the reaction with phosgene in an inert solvent of a polyamine mixture obtained by condensation of aniline...
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5354432 |
Process for the production of isocyanates and for working up the residue
A process for the production of pure distilled isocyanates in which the corresponding amine is reacted with phosgene in a suitable solvent and working up of the isocyanate containing solution...
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5349082 |
Toluene diisocyanate residue
Disclosed herein is a process for recovering toluene diisocyanate (TDI) from a TDI residue solution, comprising mixing the residue solution with a polyisocyanate consisting essentially of...
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5314588 |
Process for recovering polysocyanates from the distillation residues obtained in the production of tolylene diisocyanate
A process for recovering a distillate of tolylene diisocyanate and an isocyanate-group-containing sump product containing less than 200 ppm (by weight) tolylene diisocyanate from A) distillation...
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5312971 |
Color reduction of polymethylene polyphenyl polyisocyanates
The present invention is directed to a process for the production of polymethylene polyphenyl polyisocyanates by phosgenating the corresponding polyamines in solution in an inert organic solvent,...
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5300616 |
Process for isolating polyisocyanate isomers from polyisocyanate mixtures
Polyisocyanate mixtures are isolated in pure or more concentrated form from isomeric mixtures by liquid-liquid extraction using a two-phase system. The two phases are 1) a non-polar solvent phase...
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5298431 |
Process for producing low viscosity isocyanate trimers
This invention relates to a multi-step process for isolating a cyclotrimerized isocyanate from mixture containing said cyclotrimerized isocyanate plus an isocyanate oligomer which comprises the...
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5284969 |
Process for the production of polyisocyanates
A process for the continuous catalyst-free production of polyisocyanates by thermal decomposition of the N-substituted carbamic acid esters corresponding to the polyisocyanates, in which the...
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