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7517514 |
Process for treating residue of organic material
A process for treating organic material, separating calcium and recovering phosphorus and to utilization of the obtained products and their use as a soil conditioner and a fertilizer as well as for...
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7470414 |
High purity phosphoric acid and process of producing the same
High purity phosphoric acid having an Sb content of 200 ppb or less and a sulfide ion content of 200 ppb or less as impurity contents on a 85 weight percent H 3 PO 4 basis. The high purity...
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7378070 |
Phosphorous pentoxide producing methods
A phosphorous pentoxide producing method includes forming a kiln bed using feed agglomerates with a calcium-to-silica mole ratio of less than 1.0 and maintaining a bed temperature at or above...
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7083768 |
Processes for purifying phosphoric acid and for preparing phosphoric acid
A process for purifying phosphoric acid includes removing volatile components from phosphoric acid rich in impurities to form a crude phosphoric acid liquid substantially free of volatile...
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7070747 |
Process of eluting and recovering phosphorus from sludge
In a process of eluting phosphorus from sludge into a liquid phase and recovering the phosphorus efficiently, cell walls of microorganisms in the sludge are ruptured by a process selected from...
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6921520 |
Process for upgrading raw phosphate ore
The present invention is a process for upgrading feedstock prepared from raw phosphate ore. Phosphorus sludge is burned to produce impure phosphoric acid and the acid is combined with beneficiated...
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6861039 |
Method for purification of phosphoric acid high purity polyphosphoric acid
The present invention provides a purification method of phosphoric acid, which includes bringing phosphoric acid containing arsenic into contact with hydrogen halide, thereby to remove the arsenic...
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6814949 |
Process for production of phosphoric acid by crystallization of phosphoric acid hemihydrate
The invention relates to a process for producing simultaneously food-grade and fodder-grade phosphoric acid by crystallizing phosphoric acid hemihydrate, H 3 PO 4 ×0.5H 2 O, from a prepurified...
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6540969 |
Preparation of hexafluorophosphoric acid
The present invention provides a process for preparing hexafluorophosphoric acid complexed with about 1 to 3.3 molecules of water which are stable at temperatures below 20° C. and the compositions...
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6153552 |
Methods for making catalysts
Catalysts that are useful for hydrocarbon conversions and oxygenate conversions, and a method for making such catalysts. The method for making the catalysts comprises forming a mixture comprising...
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6002065 |
Kits for preparing calcium phosphate minerals
Setting times of calcium phosphate cement compositions are enhanced by the addition of phosphate or carbonate lubricant compositions. Methods for preparing the cement compositions are provided.
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5820632 |
Prepared calcium phosphate composition and method
Setting times of calcium phosphate cement compositions are enhanced by the addition of phosphate or carbonate lubricant compositions. Methods for preparing the cement compositions are provided.
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5580623 |
Storage stable partially neutralized acid compositions and uses
Methods and compositions are provided for preparing storage stable partially neutralized acid compositions. The partially neutralized acid compositions are amenable to prolonged periods of storage....
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5368832 |
Zero discharge process for manufacturing of phosphorous acid and hypophosphorous acid
Disclosed is a method of making phosphorous acid or hypophosphorous acid by reacting hydrogen chloride with a sodium phosphite or a sodium hypophosphite, respectively, in the presence of water to...
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5368741 |
Treatment of aqueous phosphorus wastes
Aqueous phosphorus wastes from the electric furnace production of phosphors and containing heavy metal bearing particulates are treated with lime whereby the phosphorus is converted into useful...
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5336264 |
Situ prepared calcium phosphate composition and method
Setting times of calcium phosphate cement compositions are enhanced by the addition of phosphate or carbonate lubricant compositions. Methods for preparing the cement compositions are provided.
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5275639 |
Recovery of phosphates from elemental phosphorus bearing wastes
A process for oxidizing aqueous elemental phosphorus containing residues (sludges) to produce orthophosphate containing slurries suitable for subsequent reaction with ammonia to produce nitrogen-...
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5208000 |
Hydrolysis of phosphorus trichloride
There is disclosed a process for the controlled hydrolysis of phosphorus trichloride which avoids the formation of lower oxides of phosphorus, phophines and diphosphines wherein phosphorus...
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4980142 |
Preparation of phosphorous acid
Phosphorous acid is formed by gaseous phase oxidation of phosphorus with water vapour to form predominantly P 2 O 3 and dissolving the P 2 O 3 so-formed in water. The P 2 O 3 also can be...
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4932993 |
Batch production of suspension fertilizers using lignosulfonate
In the production of suspension fertilizers the addition of an additive comprising lignosulfonate to the wet-process acid prior to the ammoniation step prevents severe thickening of the suspension...
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4919906 |
Processes and equipment for production of elemental phosphorus and thermal phosphoric acid
New processes and equipment are disclosed for producing elemental phosphorus and thermal phosphoric acid. Benefits are listed below. 1. Phosphorus-containing solids are recycled to smelting...
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4874593 |
Conversion of pyrophoric P.sub.4 -containing material to P.sub.2 O.sub.5 material
A process for treating a pyrophoric P 4 -containing material to convert it to a substantially non-pyrophoric P 2 O 5 material is described. The process comprises supplying streams of fluid P 4 ...
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4834960 |
Process for purifying phosphorous acid
The purification of phosphorous acid which is formed in halogenations of hydrocarbon derivatives using phosphorus trihalides is carried out in the context of preparing phosphorous acid in a...
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4780294 |
Process for making crude phosphoric acid
Crude phosphoric acid is made by subjecting crude phosphate ore containing sulfide to processing treatment with a mineral acid in a closed system comprised of a processing reactor, a filtering zone...
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4713228 |
Heat recovery in the manufacture of phosphorus acids
Heat is recovered from the phosphorus combustion chamber of a furnace phosphoric acid plant by placing in the combustion chamber a heat exchange surface having a protective meta acid coating...
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4698216 |
Production of an aqueous phosphoric acid solution
Aqueous phorphoric acid solutions are produced by contacting an elemental phosphorus-containing material with an oxygen-containing gas, while both are finely divided and well mixed together in a...
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4692323 |
Process for separation of magnesium-based, and possibly fluorine-and aluminum-based impurities from a wet-produced phosphoric acid
The invention concerns a process for separating magnesium-based impurities contained in a wet-process produced phosphoric acid. This process comprises adding an ammonium compound R(NH 4 ) soluble...
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4686094 |
Treatment of pyrophoric elemental phosphorus-containing material
Pyrophoric elemental phosphorus-containing material, e.g., solid waste containing high levels of elemental phosphorus (P 4 ), is treated by contact with an oxygen-containing gas, such as air, to...
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4684512 |
Phosphate recovery from wet phosphoric acid purification process
The invention is a process for recovering phosphorus value from magnesium pyrophosphate containing filter media in the wet superphosphoric acid purification process. The invention comprises...
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4639359 |
Process of removing cationic impurities from wet process phosphoric acid
A method of removing aluminum, magnesium, iron and other impurities from wet process phosphoric acid is provided. The method comprises partially ammoniating the acid and reacting the acid with a...
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4637921 |
Process for producing ammonium polyphosphate
An improved process of concentrating wet process phosphoric acid by continuously contacting an acid feed containing at least about 56 weight percent of P 2 O 5 based on the total weight of the...
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4632814 |
Process for stabilizing phosphoric acid
An improved process for stabilizing wet process phosphoric acid is described in which the acid is treated with pressurized carbon dioxide and then is aged so as to enhance the rate of...
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4619819 |
Phosphoric acid composition
Processes and compositions of matter are disclosed for the production of liquid fertilizers wherein wastewater from a phosphorus smelting furnace is incorporated in liquid fertilizer processes. The...
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4603039 |
Process for making phosphorus pentoxide and optionally phosphoric acid with utilization of the reaction heat
The disclosure relates to a process for making phosphorus pentoxide by subjecting elemental yellow phosphorus to combustion with dried air inside a steel-made combustion chamber with utilization of...
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4554144 |
Removal of magnesium and/or aluminum values from impure aqueous phosphoric acid
Magnesium and aluminum impurities are removed from aqueous phosphoric acid by treatment with a fluorine material and an alkali metal containing material in such a manner that the atomic ratio of...
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4551319 |
Two-stage concentration for superphosphoric acid
A process for the concentration of phosphoric acid by evaporation under vacuum in two stages to produce superphosphoric acid, the pressure inside the exchanger is kept equal to or greater than 0.35...
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4521392 |
Process for blending phosphoric acids of differing impurity content
Phosphoric acids of significantly different content of soluble impurities, especially magnesium compounds, can be blended to produce a phosphoric acid with a decreased tendency for forming...
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4500502 |
Process for removing impurities from wet process of phosphoric acid
A method of preparing a purified ammoniated phosphoric acid composition, comprising, reacting an aqueous wet process phosphoric acid with an ammonium ion source at a N/P 2 O 5 weight ratio...
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4495165 |
Method of purification of phosphoric acid
Appreciable inorganic impurities and organic matter are removed from impure phosphoric acid, particularly wet-process phosphoric acid, by pyrolysis of a mixture containing the raw acid and porous...
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4487750 |
Stabilization of wet process phosphoric acid
An improved method for producing wet process phosphoric acid with low post-precipitation characteristics from an unclarified dilute wet process phosphoric feed acid is described. The feed acid is...
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4483838 |
Treatment of contaminated phosphoric acid to recover usable acid therefrom
Phosphoric acid containing organic contaminants, such as phosphoric acid recovered from a thiophenol process, is treated to recover usable acid by conducting a hot separation of the contaminated...
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4442081 |
Process for producing a stabilized phosphoric acid
A wet process phosphoric acid which has been treated with aluminosilicate after the first stage of clarification can be further stabilized against precipitation of solids during storage and...
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4439407 |
Method for improving filterability of gypsum and wet process phosphoric acid
A process for the improved filterability of wet process phosphoric acid which comprises maintaining the ratio of ferric ion to ferrous ion in the wet process phosphoric acid above about 1.0 when...
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4418019 |
Process for the manufacture of 1-aminoalkane-1,1-diphosphonic acids
The invention relates to a process for making 1-aminoalkane-1,1-diphosphonic acids of the general formula (I): ##STR1## in which R stands for an aliphatic hydrocarbon radical having from 1 to 12...
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4394360 |
Process for reducing iron in phosphoric acid solution
Iron contained in phosphoric acid solution is reduced from the trivalent to the bivalent oxidation stage. To this end, red phosphorus is used as the reductant and the reduction is effected in the...
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4377559 |
New method of disposing of the residue from the production of diaklyl phosphorochloridothionate
The invention is a method of treating the distillation residue from the production of phosphorochloridothionates which comprises draining the residue into agitated cold water to form a slurry and...
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4364911 |
Method for treating the residue from the production of phosphorochloridothionates
The invention pertains to a method of treating the distillation residue from the production of phosphorochloridothionates on a continuous or semi-continuous basis. The method comprises, agitating...
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4355010 |
Process for removing phosphorus in vapor form and phosphanes from gas mixtures
Phosphorus in vapor form and phosphanes are separated from gas mixtures which consist of carbon monoxide, with or without hydrogen, nitrogen and steam. Concerned are more particularly the off-gases...
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4309394 |
Method of preparing ultraphosphoric acid
Ultraphosphoric acid containing a phosphorus to hydrogen ratio of greater than 1 can be prepared by bringing together in a reaction zone elemental phosphorus and a sufficient amount of oxygen in a...
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4301131 |
Oxidation of phosphoric acid plus K compound addition
This invention is directed to an improvement in the Hill phosphoric acid process, whereby the Hill process can be used with high-iron phosphate rock. The improvement involves oxidation of divalent...
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