Next Patent: Microfluidic device and method for producing the same
Next Patent: Microfluidic device and method for producing the same
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[0001] The present invention relates to sampling. More particularly the invention relates to a method and a device for taking a sample without causing unwanted changes to the medium to be studied, but on the same time taking necessary steps to pre-process the sample to a form more suitable for the analysis carried out.
[0002] The process of sampling is an important part of any analysis or measurement where the actual analysis or measurement is made outside of the volume actually containing the process or medium to be studied.
[0003] In
[0004] Pre-processing is an important step of the sampling as it is the object to measure the process in volume
[0005] Diluting is one of the most important methods of sample pre-processing for gaseous medium. In dilution process air, or some another dilution medium, is mixed with a sample flow. The dilution ratio, i.e. ratio between dilution flow and sample flow, varies quite a lot depending e.g. of the analysis method to be used. For example in flue gas analysis dilution rations 10-100 are commonly used. Dilution ratio is one of the major parameters to keep track on because it has direct effect on the measurement result as the measurement is made on the diluted sample.
[0006] Another important parameter of pre-processing is temperature. This is especially important when analysed gaseous samples prone for chemical reactions or vapour condensation. These kind of measurement comprise e.g. exhaust gas measurement.
[0007] Thus a good sample pre-processing process for a hot gaseous medium would be such that it would allow good control over dilution ratio and temperature.
[0008] The prior art solutions include use of diluters based on porous tubes. One example is presented in
[0009] One problem of the prior art porous tube diluters is the difficulty to adjust the dilution ration with a high precision. Also controlling the temperature of the diluted flow is difficult with a prior art porous tube dilutor.
[0010] In
[0011] It is an object of this invention to overcome the disadvantages of the prior art. With an embodiment according to this invention the dilution process is easier to control and have fewer losses than the prior art solutions.
[0012] In an embodiment of the invention a sample flow is first diluted with a porous tube type dilution configuration and after that with an ejector type dilution configuration.
[0013] In another embodiment the transition delay between said two dilution configurations is so short that uncontrolled transformation of the sample are minimised.
[0014] In further embodiment the porous tube type dilution configuration comprise two flow guides, one for dilution medium and another for cooling medium. These flow guides are separated by a wall comprising heat exchange means. These heat exchange means could comprise serrate shaped structures strengthening the heat exchange effect.
[0015] In the following a present invention will be described in more detail with the reference to the appended figures, in which
[0016]
[0017]
[0018]
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[0020]
[0021]
[0022] In this text a term diluter is used, but that is not to be intended as limiting the scope of protection only to the devices called as diluters. It is e.g. possible to manufacture a single device comprising both the sample pre-processing and analysing and call that device an analyser, but still fall under the scope of this application. Thus the actual term used to call the device is not significant. What matters is the device comprising the parts identified in the accomplishing claims or their equivalents.
[0023] In
[0024] Carrying out the dilution in two phases gives clear benefits over the prior art solutions. Losses would be low because the first dilution flow
[0025] The low losses are, however, achieved without sacrificing accuracy of controlling of the dilution ration and temperature as would be the case if prior art type solution based on a porous tube diluter would be used. As the second dilution is carried out by a ejector type configuration these parameter are easily controlled.
[0026] In one embodiment said two dilution phases are carried out so close to each other that there is no time for significant changes of characteristics like temperature of chemical composition the sample flow to happen. That is to say that the transition delay between two dilution phases is short compared to the uncontrolled transformations happening in the sample. One way of achieving this would be to place the porous tube type configuration and ejector type configuration so close to each other that the means connecting them could be short compared to the velocity of the flow.
[0027] The means carrying out the first and second dilution can be arranged so that the exit opening of the porous tube type construction would be entry opening for a ejector type construction. Said two construction could be build e.g. to a single case forming one combined device.
[0028] As the first and second dilution flows have slightly different objectives, in one embodiment of the invention said first dilution flow
[0029] If
[0030] To improve heat exchange between said first and second flow guides, one or both sides of the wall separating said two flow guides can be equipped with a geometry improving heat exchange, like a serrate shaped structures
[0031] It is to be understood that although the present invention has been specially disclosed with preferred embodiments and examples, modifications to these may be apparent to a man skilled in the art and such modifications and variations are considered to be within the scope of the invention and the appended claims. It is also intended that all the matter contained in the above description shall be interpreted as illustrative and not in a limiting sense.